7XLJ
The crystal structure of ORE1(ANAC092) NAC domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-03-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9794 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.333, 73.761, 78.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.880 - 2.450 |
R-factor | 0.2192 |
Rwork | 0.217 |
R-free | 0.26240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ulx |
RMSD bond length | 0.009 |
RMSD bond angle | 1.092 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.17.1_3660) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.880 | 2.540 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.048 | 0.488 |
Number of reflections | 15181 | 1301 |
<I/σ(I)> | 26.58 | 1.77 |
Completeness [%] | 98.5 | 86.1 |
Redundancy | 6.9 | 4.9 |
CC(1/2) | 0.998 | 0.907 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1M tris pH 8.5, 7% PEG20K |