7XH0
crystal structure of Csn-PD from Paenibacillus dendritiformis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-27 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.18071 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 68.510, 73.138, 99.975 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.720 - 1.680 |
Rwork | 0.150 |
R-free | 0.19510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2d05 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.639 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.720 | 1.710 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.052 | 0.446 |
Number of reflections | 28796 | 1417 |
<I/σ(I)> | 21.7 | |
Completeness [%] | 99.4 | |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Citric acid pH3.5, 25% PEG3,350 |