7XEX
Crystal strucutre of apoCasDinG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-19 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 264.828, 72.232, 139.428 |
Unit cell angles | 90.00, 121.22, 90.00 |
Refinement procedure
Resolution | 38.370 - 3.000 |
R-factor | 0.2156 |
Rwork | 0.213 |
R-free | 0.26020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fwr |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1-4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 44576 | 4125 |
<I/σ(I)> | 12 | |
Completeness [%] | 98.1 | |
Redundancy | 6.7 | |
CC(1/2) | 0.845 | 0.845 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 8% PEG 6000, 0.1M HEPES 7.4 |