7XBH
The complex structure of RshSTT182/200 RBD bound to human ACE2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-06-21 |
| Detector | DECTRIS EIGER2 S 9M |
| Wavelength(s) | 0.979183 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 155.413, 155.229, 60.996 |
| Unit cell angles | 90.00, 103.66, 90.00 |
Refinement procedure
| Resolution | 29.640 - 3.020 |
| R-factor | 0.2023 |
| Rwork | 0.201 |
| R-free | 0.23460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6lzg |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.589 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19rc3_4028) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.420 | 2.920 |
| High resolution limit [Å] | 2.720 | 2.720 |
| Rmerge | 0.166 | 2.842 |
| Number of reflections | 37596 | 2783 |
| <I/σ(I)> | 9.4 | 0.9 |
| Completeness [%] | 99.8 | |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.01M sodium borate pH 8.5, 1.0M sodium citrate |
