7X9Z
Thermotoga maritima ferritin variant-Tm-E(G40E) with Co
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-03 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 1.597735 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.517, 65.809, 91.064 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.340 - 2.290 |
R-factor | 0.1939 |
Rwork | 0.188 |
R-free | 0.24640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vlg |
Data reduction software | DIALS |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.340 | 2.372 |
High resolution limit [Å] | 2.290 | 2.290 |
Number of reflections | 29843 | 2470 |
<I/σ(I)> | 13.89 | |
Completeness [%] | 98.6 | |
Redundancy | 2 | |
CC(1/2) | 0.991 | 0.976 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 25mM HEPES, pH 8.0, 55% MPD, 5mM Cobalt chloride |