7X7S

Solution structure of human adenylate kinase 1 (hAK1)

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	UNITY		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D C(CO)NH
11	1	2	3D 1H-13C NOESY
12	1	2	3D 1H-15N NOESY
2	1	2	3D HNCACB
3	1	2	3D CBCA(CO)NH
4	1	2	3D HNCA
5	1	2	3D HN(CO)CA
6	1	2	3D HNCO
7	1	2	3D 1H-15N TOCSY
8	1	2	3D HBHA(CO)NH
9	1	2	3D HCCH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.2	1	298

Conformers

Conformers Calculated Total Number	300
Conformers Submitted Total Number	20