7X4F
Native CD-NTase LpCdnE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-11-10 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.000 |
Spacegroup name | P 31 |
Unit cell lengths | 60.507, 60.507, 100.588 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.970 - 2.460 |
R-factor | 0.1928 |
Rwork | 0.191 |
R-free | 0.22320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7x4a |
RMSD bond length | 0.003 |
RMSD bond angle | 0.483 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.540 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.077 | 0.629 |
Rpim | 0.047 | 0.378 |
Number of reflections | 14892 | 1507 |
<I/σ(I)> | 16.5 | 2.1 |
Completeness [%] | 99.0 | 100 |
Redundancy | 3.7 | 3.8 |
CC(1/2) | 0.652 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | MgCl2, Tris, PEG 8000 |