7WZ5
Larimichthys crocea IFNi
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-06-19 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 0.979176 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.310, 60.620, 81.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.150 - 1.390 |
R-factor | 0.1993 |
Rwork | 0.199 |
R-free | 0.21280 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3piw |
RMSD bond length | 0.006 |
RMSD bond angle | 0.829 |
Data reduction software | xia2 (1.0) |
Data scaling software | xia2 (1.0) |
Phasing software | PARROT (1.0) |
Refinement software | PHENIX (1.13) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.000 | 1.430 |
High resolution limit [Å] | 1.390 | 1.390 |
Number of reflections | 36077 | 36077 |
<I/σ(I)> | 30.97 | |
Completeness [%] | 97.8 | |
Redundancy | 5 | |
CC(1/2) | 0.997 | 0.708 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 289.15 | Calcium chloride dihydrate, BIS-TRIS, Polyethylene glycol monomethyl ether 550 |