7WW4
Crystal structure of multidomain beta-1,3(4)-glucanase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-10 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.9792 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 120.940, 120.940, 70.050 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.527 - 2.230 |
R-factor | 0.249873564816 |
Rwork | 0.248 |
R-free | 0.28521 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.466 |
Data scaling software | HKL-3000 |
Refinement software | PHENIX (dev_2474) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.530 | 2.310 |
High resolution limit [Å] | 2.230 | 2.230 |
Rmeas | 0.136 | |
Number of reflections | 28796 | 2685 |
<I/σ(I)> | 17.7 | |
Completeness [%] | 98.0 | |
Redundancy | 7.2 | |
CC(1/2) | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.056M sodium phosphate monobasic monohydrate, 1.344M potassium phosphate dibasic |