7WVT
Crystal structure of Saccharomyces cerevisiae Sfh2 complexed with phosphatidylinositol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2021-07-26 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97950 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.541, 117.132, 42.555 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.770 - 1.500 |
R-factor | 0.1702 |
Rwork | 0.169 |
R-free | 0.21150 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.967 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.084 | 0.284 |
Number of reflections | 59663 | 2577 |
<I/σ(I)> | 40.1 | 5.6 |
Completeness [%] | 98.0 | 85.6 |
Redundancy | 4.8 | 2.4 |
CC(1/2) | 0.996 | 0.898 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 0.1 M MES pH 6.0, 30% PEG 1000 |