7WVR
Crystal structure of Talaromyces leycettanus JCM12802 expansin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 47.862, 117.627, 99.203 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.300 - 1.410 |
R-factor | 0.1622 |
Rwork | 0.161 |
R-free | 0.17560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jcw |
RMSD bond length | 0.005 |
RMSD bond angle | 0.792 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.300 | 1.457 |
High resolution limit [Å] | 1.407 | 1.407 |
Rmerge | 0.329 | |
Rmeas | 0.466 | |
Number of reflections | 50454 | 3433 |
<I/σ(I)> | 16.48 | 2.34 |
Completeness [%] | 92.3 | |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.785 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.8 M ammonium sulfate, 0.1 M Bis-Tris (pH 6.5), and 2% PEG monomethyl ether 550 |