7WUC
Room-temperature structure of lysozyme by serial femtosecond crystallography (BITS)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | PAL-XFEL BEAMLINE NCI |
Synchrotron site | PAL-XFEL |
Beamline | NCI |
Temperature [K] | 298.15 |
Detector technology | CCD |
Collection date | 2021-12-23 |
Detector | RAYONIX MX225-HS |
Wavelength(s) | 1.30 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.480, 79.480, 38.480 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.740 - 2.100 |
R-factor | 0.2228 |
Rwork | 0.220 |
R-free | 0.24890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7wkr |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 2.170 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 7605 | 724 |
<I/σ(I)> | 7.38 | |
Completeness [%] | 100.0 | |
Redundancy | 590.7 | |
CC(1/2) | 0.987 | 0.477 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 298.5 | Na-acetate, NaCl, PEG 8000 |