7WN7
Crystal structure of HearNPV P26
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9778 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 194.749, 69.236, 52.746 |
Unit cell angles | 90.00, 102.18, 90.00 |
Refinement procedure
Resolution | 28.740 - 1.900 |
R-factor | 0.1849 |
Rwork | 0.184 |
R-free | 0.21060 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19_4080) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.970 |
High resolution limit [Å] | 1.900 | 4.090 | 1.900 |
Rmerge | 0.072 | 0.046 | 0.339 |
Rmeas | 0.081 | 0.052 | 0.375 |
Rpim | 0.035 | 0.023 | 0.157 |
Total number of observations | 253451 | ||
Number of reflections | 52908 | 5485 | 5114 |
<I/σ(I)> | 5.1 | ||
Completeness [%] | 97.1 | 98.4 | 94.7 |
Redundancy | 4.8 | 4.7 | 4.6 |
CC(1/2) | 0.996 | 0.952 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.7 | 289 | PEG MME 5000 |