7WEG
Complex structure of PDZD7 and FCHSD2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-04 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.978460 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.603, 62.918, 46.030 |
Unit cell angles | 90.00, 95.19, 90.00 |
Refinement procedure
Resolution | 19.680 - 2.000 |
R-factor | 0.2136 |
Rwork | 0.209 |
R-free | 0.25560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vrf |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.680 | 19.680 | 2.060 |
High resolution limit [Å] | 2.000 | 8.960 | 2.000 |
Rmerge | 0.125 | 0.055 | 0.715 |
Rmeas | 0.136 | 0.059 | 0.774 |
Total number of observations | 106495 | ||
Number of reflections | 15785 | 174 | 1120 |
<I/σ(I)> | 10.01 | 26.95 | 3 |
Completeness [%] | 98.6 | 89.7 | 95.5 |
Redundancy | 6.747 | 6.489 | 6.727 |
CC(1/2) | 0.997 | 0.997 | 0.915 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.05M Zinc acetate dehydrate, 20% w/v polyethylene glycol 3350 |