7WDR
Crystal structures of MeBglD2 in complex with various saccharides
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-05 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.9 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 201.847, 201.847, 201.847 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.000 |
R-factor | 0.18929 |
Rwork | 0.187 |
R-free | 0.24235 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xgz |
RMSD bond length | 0.010 |
RMSD bond angle | 1.778 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.136 | 0.777 |
Number of reflections | 46907 | 2294 |
<I/σ(I)> | 10.5 | |
Completeness [%] | 99.5 | |
Redundancy | 12.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl buffer (pH 8.5), 1.2 M lithium sulfate, 0.01 M nickel chloride |