7WBG
BF2*1901/RY8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.127, 85.025, 110.838 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.400 - 2.000 |
R-factor | 0.1856 |
Rwork | 0.183 |
R-free | 0.23580 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yez |
RMSD bond length | 0.007 |
RMSD bond angle | 0.906 |
Data scaling software | HKL-2000 |
Phasing software | PHASER (1.13_2998) |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.068 | 0.142 |
Number of reflections | 49775 | 4913 |
<I/σ(I)> | 13.1 | |
Completeness [%] | 98.2 | |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.15 M Potassium bromide and 30% w/v Polyethylene glycol monomethyl ether 2,000 |