7WA9
Crystal structure of MSMEG_5634 from Mycobacterium smegmatis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2017-07-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 71.072, 55.011, 40.733 |
Unit cell angles | 90.00, 112.75, 90.00 |
Refinement procedure
Resolution | 22.190 - 1.900 |
R-factor | 0.2357 |
Rwork | 0.233 |
R-free | 0.28210 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.095 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.098 | 0.596 |
Number of reflections | 21971 | 1149 |
<I/σ(I)> | 33.3 | |
Completeness [%] | 98.3 | |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293 | 0.2 M Calcium acetate hydrate, 20% w/v Polyethylene Glycol 3350, pH 7.5 |