7W83

Structure of the C-terminal head domain of the fowl adenovirus type 4 fiber 2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 4.2.2
Synchrotron site	ALS
Beamline	4.2.2
Temperature [K]	273
Detector technology	CCD
Collection date	2021-10-17
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.97
Spacegroup name	P 63
Unit cell lengths	60.340, 60.340, 192.600
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.480 - 1.290
R-factor	0.187
Rwork	0.185
R-free	0.22100
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2vtw
RMSD bond length	0.014
RMSD bond angle	1.694
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	REFMAC (5.8.0230)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.480	1.320
High resolution limit [Å]	1.290	1.290
Number of reflections	98150	6455
<I/σ(I)>	16.8
Completeness [%]	98.8
Redundancy	17.3
CC(1/2)	0.998	0.741

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		293	0.1 M Sodium acetate trihydrate pH 7.0 12% w/v Polyethylene glycol 3,350