7W70
Crystal structure of the PDZ-C domain fragment of Kangiella koreensis RseP orthologue
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-22 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9800 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.673, 42.408, 97.949 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.290 - 1.150 |
R-factor | 0.1967 |
Rwork | 0.196 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zpm |
RMSD bond length | 0.006 |
RMSD bond angle | 0.822 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.410 | 1.170 |
High resolution limit [Å] | 1.150 | 1.150 |
Rpim | 0.017 | 0.350 |
Number of reflections | 60798 | 2913 |
<I/σ(I)> | 17.1 | 2.2 |
Completeness [%] | 99.6 | |
Redundancy | 6.4 | |
CC(1/2) | 0.999 | 0.794 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 1.0 M ammonium sulfate, 0.1 M HEPES-Na (pH 7.5) |