7W09
UGT74AN2, Plant Steroid Glycosyltransferase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-26 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979150 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.413, 75.446, 61.766 |
Unit cell angles | 90.00, 113.84, 90.00 |
Refinement procedure
Resolution | 30.400 - 1.950 |
R-factor | 0.2033 |
Rwork | 0.202 |
R-free | 0.23570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6l8z |
RMSD bond length | 0.008 |
RMSD bond angle | 0.896 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.770 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.107 | |
Rmeas | 0.126 | |
Rpim | 0.067 | |
Number of reflections | 32926 | 2268 |
<I/σ(I)> | 10.3 | 2.9 |
Completeness [%] | 98.8 | 97.4 |
Redundancy | 6.7 | 6.3 |
CC(1/2) | 0.996 | 0.866 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | PEG 3350, sodium chloride, MES (pH 6.5) |