7VWS

Carbazole Prenyl Transferase LvqB4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Temperature [K]	93.15
Detector technology	PIXEL
Collection date	2019-10-11
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.999999
Spacegroup name	P 1 21 1
Unit cell lengths	63.240, 71.394, 83.894
Unit cell angles	90.00, 109.91, 90.00

Refinement procedure

Resolution	45.690 - 1.710
R-factor	0.1779
Rwork	0.176
R-free	0.21330
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	Se-SAD
RMSD bond length	0.006
RMSD bond angle	0.761
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.690	1.771
High resolution limit [Å]	1.710	1.710
Number of reflections	68798	18243
<I/σ(I)>	9.43
Completeness [%]	89.5
Redundancy	6.3
CC(1/2)	0.913	0.627

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		277.15	PEG 3350