7VWO
TA complex from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 50.847, 74.501, 74.882 |
Unit cell angles | 73.16, 70.24, 70.03 |
Refinement procedure
Resolution | 44.550 - 2.000 |
R-factor | 0.2036 |
Rwork | 0.201 |
R-free | 0.24685 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.936 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.550 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.048 | |
Rmeas | 0.064 | |
Rpim | 0.042 | |
Number of reflections | 59128 | 8216 |
<I/σ(I)> | 5.1 | |
Completeness [%] | 95.7 | |
Redundancy | 2 | |
CC(1/2) | 0.996 | 0.323 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M Potassium chloride, 0.1 M Magnesium acetate tetrahydrate 0.05 M Sodium cacodylate trihydrate pH 6.5 10% w/v Polyethylene glycol 8,000 |