7VUD
Carotenoid Cleavage Dioxygenase 1 from Osmanthus fragrans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 98.15 |
Detector technology | CCD |
Collection date | 2021-02-24 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 209.941, 209.941, 209.941 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.480 - 2.800 |
Rwork | 0.227 |
R-free | 0.25840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3npe |
RMSD bond length | 0.006 |
RMSD bond angle | 1.451 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.530 | 2.910 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.015 | 0.320 |
Number of reflections | 39479 | 4387 |
<I/σ(I)> | 10.8 | 1.1 |
Completeness [%] | 100.0 | |
Redundancy | 81 | |
CC(1/2) | 0.996 | 0.380 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293.15 | 0.1M Tris pH 7.5, 1.5M Ammonium Sulfate |