7VU2
Chitoporin from Serratia marcescens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97886 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 82.967, 82.967, 189.526 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 62.423 - 1.850 |
R-factor | 0.1742 |
Rwork | 0.173 |
R-free | 0.19730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7vu0 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.760 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.101 | |
Number of reflections | 57273 | 57273 |
<I/σ(I)> | 24.8 | |
Completeness [%] | 100.0 | |
Redundancy | 11.7 | |
CC(1/2) | 0.993 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | PEG 8000, calcium acetate, MES pH 6.0 |