7VTM
Crystal structure of Glucoside hydrolase family 64 beta-1,3-glucanase complexed with Laminaritetraose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-01-01 |
Detector | DECTRIS EIGER2 X 1M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 79.486, 79.486, 156.662 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.110 - 2.052 |
R-factor | 0.21204109066 |
Rwork | 0.211 |
R-free | 0.22808 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7vtk |
RMSD bond length | 0.014 |
RMSD bond angle | 1.227 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_2474) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.110 | 2.100 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.011 | |
Rmeas | 0.009 | |
Number of reflections | 36584 | 36584 |
<I/σ(I)> | 31.4 | |
Completeness [%] | 97.0 | |
Redundancy | 19.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.1M sodium malonate pH 7.0, 0.1M HEPES pH 7.0 |