7VRX
Pad-1 in the absence of substrate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2020-11-12 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97933 |
Spacegroup name | P 65 |
Unit cell lengths | 96.157, 96.157, 407.132 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.856 - 1.966 |
R-factor | 0.253754535002 |
Rwork | 0.253 |
R-free | 0.29055 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o4s |
RMSD bond length | 0.006 |
RMSD bond angle | 1.110 |
Data reduction software | HKL-2000 (706e) |
Data scaling software | HKL-2000 (706e) |
Phasing software | PHASER (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.040 |
High resolution limit [Å] | 1.960 | 1.970 |
Number of reflections | 149234 | 14983 |
<I/σ(I)> | 18.705 | |
Completeness [%] | 99.3 | |
Redundancy | 10.7 | |
CC(1/2) | 0.990 | 0.396 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.1 M sodium acetate (pH 4.6), 1.8 M ammonium sulfate |