7VRR
Crystal structure of Arabidopsis thaliana HDT1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 103 |
Detector technology | CCD |
Collection date | 2018-01-14 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.979470 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.961, 79.961, 143.625 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.110 - 2.950 |
Rwork | 0.224 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7vmf |
RMSD bond length | 0.009 |
RMSD bond angle | 1.315 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.420 | 3.130 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.108 | 0.637 |
Rmeas | 0.120 | |
Number of reflections | 10405 | 1621 |
<I/σ(I)> | 20.2 | 4.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.7 | 10.1 |
CC(1/2) | 0.998 | 0.928 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 301 | 50 mM MgCl2.6H2O, 0.1M HEPES (pH 7.5), 30% V/V PEG MME 550 |