7VQA
Structure of MA1831 from Methanosarcina acetivorans in complex with dimethylallyl diphosphate.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | LIQUID ANODE |
Source details | BRUKER METALJET |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-08 |
Detector | Bruker PHOTON III |
Wavelength(s) | 1.34138 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 111.848, 81.567, 60.044 |
Unit cell angles | 90.00, 103.74, 90.00 |
Refinement procedure
Resolution | 33.450 - 1.790 |
R-factor | 0.155 |
Rwork | 0.152 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7caq |
Data reduction software | SAINT |
Data scaling software | Aimless (0.6.3) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.890 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.051 | 0.260 |
Number of reflections | 43956 | 7297 |
<I/σ(I)> | 29 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 10.9 | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | 0.5M ammonium sulfate, 0.1M Tris (pH 8.0), 12% glycerol |