7VNW
Crystal Structure of tRNAVal from Sulfolobus Tokodaii(Dephosphorylated)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-09 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.560, 116.680, 56.140 |
Unit cell angles | 90.00, 101.34, 90.00 |
Refinement procedure
Resolution | 31.920 - 2.610 |
R-factor | 0.2255 |
Rwork | 0.224 |
R-free | 0.26050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | D_1300024972 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 31.920 | 31.920 | 2.680 |
High resolution limit [Å] | 2.610 | 11.670 | 2.610 |
Rmerge | 0.111 | 0.037 | 1.151 |
Rmeas | 0.121 | 0.040 | 1.254 |
Total number of observations | 83923 | ||
Number of reflections | 12524 | 140 | 948 |
<I/σ(I)> | 14.52 | 37.57 | 1.88 |
Completeness [%] | 99.7 | 97.2 | 99.6 |
Redundancy | 6.701 | 6.586 | 6.325 |
CC(1/2) | 0.998 | 0.999 | 0.596 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 80mM NaCl, 12mM Speremin-4HCl, 30% MPD, 40mM NaCacodylate pH 6.5 |