7VKR
Crystal structure of D. melanogaster SAMTOR in complex with SAM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-04 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 50.269, 64.095, 79.274 |
Unit cell angles | 90.10, 93.27, 96.61 |
Refinement procedure
Resolution | 43.322 - 2.100 |
R-factor | 0.1896 |
Rwork | 0.188 |
R-free | 0.23870 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.007 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.322 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.127 | 0.841 |
Number of reflections | 51008 | 3585 |
<I/σ(I)> | 9.5 | 1.8 |
Completeness [%] | 88.5 | 59.6 |
Redundancy | 4.2 | 4.2 |
CC(1/2) | 0.995 | 0.602 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 289 | 0.1 M sodium citrate, pH 5.0, and 20% (w/v) PEG 8,000 |