Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-07-13 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.650, 67.150, 42.600 |
| Unit cell angles | 90.00, 106.92, 90.00 |
Refinement procedure
| Resolution | 32.960 - 1.594 |
| R-factor | 0.1536 |
| Rwork | 0.152 |
| R-free | 0.18800 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.767 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19.2-4158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 67.150 | 1.680 |
| High resolution limit [Å] | 1.590 | 1.590 |
| Number of reflections | 28345 | 4100 |
| <I/σ(I)> | 8.8 | |
| Completeness [%] | 99.4 | |
| Redundancy | 5.1 | |
| CC(1/2) | 0.994 | 0.774 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 293 | 0.1M Sodium Hepes pH 7.5, 2% PEG 400, 2.0M (NH4)2SO4 |
