7V3Q
Crystal structure of anti-MUC1 antibody 16A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2017-09-19 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.632, 126.696, 158.201 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.680 - 2.980 |
R-factor | 0.2203 |
Rwork | 0.218 |
R-free | 0.26370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4yhy |
RMSD bond length | 0.004 |
RMSD bond angle | 0.838 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.680 | 3.090 |
High resolution limit [Å] | 2.980 | 2.980 |
Rmeas | 0.184 | 0.728 |
Rpim | 0.086 | 0.350 |
Number of reflections | 18236 | 1686 |
<I/σ(I)> | 9.1 | 2.1 |
Completeness [%] | 97.7 | 92.3 |
Redundancy | 4.1 | 3.9 |
CC(1/2) | 0.970 | 0.707 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 289 | 1.0 M Lithium chloride 0.1 M Tris pH 8.5 20%(w/v) PEG 6000 |