7UYL
850 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2019-11-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.033167 |
Spacegroup name | I 41 |
Unit cell lengths | 137.180, 137.180, 63.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.160 - 2.000 |
R-factor | 0.1758 |
Rwork | 0.174 |
R-free | 0.21230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6d01 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.708 |
Data reduction software | XPREP |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.160 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 40192 | 5428 |
<I/σ(I)> | 8.55 | 1.95 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.93 | 8 |
CC(1/2) | 0.995 | 0.706 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 85 mM Tris pH 8.5, 170 mM sodium acetate, 25.5% (w/v) polyethylene glycol 4000, 15% glycerol |