7USI
BRD2-BD1 in complex with MDP5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-07-17 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.810, 149.872, 63.819 |
Unit cell angles | 90.00, 112.27, 90.00 |
Refinement procedure
Resolution | 35.560 - 2.500 |
R-factor | 0.2035 |
Rwork | 0.201 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6jke |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.560 | 2.589 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.126 | |
Rpim | 0.048 | |
Number of reflections | 38336 | 3871 |
<I/σ(I)> | 24.6 | |
Completeness [%] | 99.7 | |
Redundancy | 6.9 | |
CC(1/2) | 0.978 | 0.834 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289.15 | 0.2 M Sodium tartrate dibasic dihydrate pH 7.5 and 20 % w/v PEG 1000 |