7UQL
Pathogenesis related 10-10 app from
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.175, 92.547, 52.858 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.090 - 1.900 |
R-factor | 0.2104 |
Rwork | 0.207 |
R-free | 0.24740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ka3 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.947 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2-3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.600 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 27479 | 1977 |
<I/σ(I)> | 27.42 | |
Completeness [%] | 98.5 | |
Redundancy | 8.1 | |
CC(1/2) | 1.000 | 0.849 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, Bis-Tris pH 5.5 |