7UF0
RibB from Vibrio cholera bound with D-ribulose-5-phosphate (D-Ru5P)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 60.671, 78.625, 90.319 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.310 - 1.800 |
R-factor | 0.169 |
Rwork | 0.165 |
R-free | 0.20190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4p8e |
RMSD bond length | 0.011 |
RMSD bond angle | 1.237 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.310 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rpim | 0.048 | 0.359 |
Number of reflections | 20407 | 1209 |
<I/σ(I)> | 13 | 2.3 |
Completeness [%] | 99.9 | |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.1 M lithium acetate, 12-18% w/v PEG3350 |