7U8A
Product of 14mer primer with activated G monomer diastereomer 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 98 |
Detector technology | CCD |
Collection date | 2021-05-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 42.873, 42.873, 82.763 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.416 - 2.100 |
Rwork | 0.199 |
R-free | 0.28180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6c8o |
RMSD bond length | 0.038 |
RMSD bond angle | 2.706 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.079 | 0.527 |
Rmeas | 0.083 | 0.556 |
Rpim | 0.026 | 0.175 |
Number of reflections | 5553 | 273 |
<I/σ(I)> | 25.9 | 4.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 10.2 | 9.9 |
CC(1/2) | 0.993 | 0.935 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293.15 | 50 mM PIPES pH 7.0, 65 mM Magnesium chloride, 1 mM Cobalt (III) Hexamine chloride, 26% v/v (+/-)-2-Methyl-2,4-pentanediol |