7U88
Product of 13mer primer with activated G monomer diastereomer 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 98 |
Detector technology | CCD |
Collection date | 2021-05-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 42.723, 42.723, 85.822 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.948 - 2.140 |
Rwork | 0.214 |
R-free | 0.29160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6c8o |
RMSD bond length | 0.018 |
RMSD bond angle | 2.603 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.140 | 2.140 |
Rmerge | 0.077 | 0.402 |
Rmeas | 0.082 | 0.438 |
Rpim | 0.027 | 0.166 |
Number of reflections | 5344 | 229 |
<I/σ(I)> | 24.2 | 2.2 |
Completeness [%] | 99.2 | |
Redundancy | 9.5 | 5.7 |
CC(1/2) | 1.000 | 0.948 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293.15 | 1.5 M Lithium sulfate, 50 mM TRIS pH 8.5, 5% w/v Glycerol |