7U87
Product of 13mer primer with activated G monomer diastereomer 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 98 |
Detector technology | CCD |
Collection date | 2021-05-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 42.741, 42.741, 83.280 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.675 - 1.701 |
Rwork | 0.188 |
R-free | 0.23990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6c8o |
RMSD bond length | 0.033 |
RMSD bond angle | 3.256 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.089 | 0.348 |
Rmeas | 0.094 | 0.376 |
Rpim | 0.030 | 0.139 |
Number of reflections | 10199 | 474 |
<I/σ(I)> | 19.4 | 2.7 |
Completeness [%] | 99.9 | |
Redundancy | 9.9 | 6.5 |
CC(1/2) | 1.000 | 0.989 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293.15 | 0.2 M Ammonium acetate, 0.1 M BIS-TRIS pH 6.5, 45% v/v (+/-)-2-Methyl-2,4-pentanediol |