7U4M
Crystal structure of human GPX4-U46C in complex with LOC1886
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-28 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 67.828, 115.654, 61.219 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.510 - 1.930 |
R-factor | 0.1646 |
Rwork | 0.161 |
R-free | 0.19710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7l8k |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.220 | 1.800 |
High resolution limit [Å] | 1.770 | 1.770 |
Rmerge | 0.126 | 2.577 |
Number of reflections | 23683 | 1140 |
<I/σ(I)> | 11.4 | |
Completeness [%] | 99.1 | 84.4 |
Redundancy | 13.2 | 11.5 |
CC(1/2) | 0.998 | 0.400 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 4.6 | 291 | 2 M sodium chloride and 0.1 M sodium acetate trihydrate |