7TLN
STRUCTURAL ANALYSIS OF THE INHIBITION OF THERMOLYSIN BY AN ACTIVE-SITE-DIRECTED IRREVERSIBLE INHIBITOR
Replaces: 6TLNExperimental procedure
Spacegroup name | P 61 2 2 |
Unit cell lengths | 94.200, 94.200, 131.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.300 |
Rwork | 0.170 |
RMSD bond length | 0.021 * |
RMSD bond angle | 2.900 * |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Number of reflections | 12268 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 2 | calcium acetate | 0.01 (M) | |
2 | 1 | 2 | Tris acetate | 0.01 (M) | |
3 | 1 | 2 | dimethylsulfoxide | 5 (%(v/v)) | or 7%(v/v) |