7TJO
HIV-1 gp120 complex with CJF-II-197-S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-26 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.339, 121.826, 195.724 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.930 - 3.070 |
R-factor | 0.2326 |
Rwork | 0.229 |
R-free | 0.26790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tgr |
RMSD bond length | 0.004 |
RMSD bond angle | 0.683 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.20rc3_4406) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.350 |
High resolution limit [Å] | 3.070 | 3.070 |
Rmerge | 0.283 | |
Number of reflections | 23992 | 1200 |
<I/σ(I)> | 8.4 | |
Completeness [%] | 99.8 | |
Redundancy | 13.4 | |
CC(1/2) | 0.996 | 0.664 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 14%(w/v) PEG 1500, 0.1 M calcium chloride, 0.1 M imidazole pH 6.5 |