7TJE

Bacteriophage Q beta capsid protein A38K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Temperature [K]	100
Detector technology	CCD
Collection date	2016-10-18
Detector	RAYONIX MX300-HS
Wavelength(s)	0.979
Spacegroup name	I 2 3
Unit cell lengths	194.143, 194.143, 194.143
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.760 - 2.799
R-factor	0.2212
Rwork	0.219
R-free	0.26810
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1qbe
RMSD bond length	0.009
RMSD bond angle	1.120
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.11.1_2575)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.800	2.900
High resolution limit [Å]	2.799	2.800
Number of reflections	29445	3012
<I/σ(I)>	16.5
Completeness [%]	97.9
Redundancy	2
CC(1/2)	0.800	0.800

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	298	PEG 3350, L-proline, HEPES