7TAL
LOV2-DARPIN fusion : D4_deltaDARP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-12-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.142, 50.768, 87.263 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.880 - 1.100 |
R-factor | 0.1543 |
Rwork | 0.152 |
R-free | 0.20330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v0w |
RMSD bond length | 0.016 |
RMSD bond angle | 2.067 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.880 | 1.190 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.044 | |
Rpim | 0.013 | |
Number of reflections | 46107 | 2305 |
<I/σ(I)> | 20.9 | 1.9 |
Completeness [%] | 83.5 | 74.8 |
Redundancy | 12.4 | 9.7 |
CC(1/2) | 0.999 | 0.702 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1 M lithium sulphate, 2% PEG8000, pH undefined |