7TAK
Structure of a NAT transporter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-01-09 |
Detector | MPCCD |
Wavelength(s) | 0.9150 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 131.713, 135.993, 79.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.781 - 2.798 |
R-factor | 0.1997 |
Rwork | 0.198 |
R-free | 0.23190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xls |
RMSD bond length | 0.008 |
RMSD bond angle | 1.192 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_1951) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.031 | 2.898 |
High resolution limit [Å] | 2.798 | 2.798 |
Rmerge | 0.250 | 0.250 |
Number of reflections | 35338 | 2307 |
<I/σ(I)> | 5 | |
Completeness [%] | 98.7 | |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 277.15 | 30% (v/v) PEG 400, 0.1 M MES pH 6.0, 3 mM Na-glycochenodeoxycholate and 0.5 mM 6-bromopurine |