7SVL
DPP9 IN COMPLEX WITH LIGAND ICeD-2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX10.1 |
| Synchrotron site | SRS |
| Beamline | PX10.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-02-13 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 119.716, 117.398, 163.691 |
| Unit cell angles | 90.00, 105.60, 90.00 |
Refinement procedure
| Resolution | 157.660 - 2.460 |
| R-factor | 0.2635 |
| Rwork | 0.263 |
| R-free | 0.34090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6eoq |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.568 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 157.660 | 2.524 |
| High resolution limit [Å] | 2.460 | 2.460 |
| Rmerge | 0.103 | 0.597 |
| Number of reflections | 151376 | 11309 |
| <I/σ(I)> | 6.1 | |
| Completeness [%] | 95.6 | 97.28 |
| Redundancy | 1.9 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 10% PEG 8000 25% Glycerol 0.16 M Calcium Acetate 0.08 M Cacodilate pH 6.25 |
