Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

7SPY

Get3 bound to ATP from G. intestinalis in the closed form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL12-2
Synchrotron siteSSRL
BeamlineBL12-2
Temperature [K]100
Detector technologyPIXEL
Collection date2021-07-15
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.97946
Spacegroup nameP 32 2 1
Unit cell lengths79.646, 79.646, 130.070
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution43.390 - 2.230
R-factor0.17929
Rwork0.178
R-free0.20886
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3ibg
RMSD bond length0.006
RMSD bond angle1.313
Data reduction softwareHKL-3000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.270
High resolution limit [Å]2.2302.230
Rpim0.0350.453
Number of reflections233011163
<I/σ(I)>22.56
Completeness [%]97.4
Redundancy8.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.1 M Tris, pH 7.5, 0.2 M ammonium sulfate, 15% PEG3350

223166

PDB entries from 2024-07-31

PDB statisticsPDBj update infoContact PDBjnumon