7SLJ

[U:Ag+:U--pH 8.5] Metal-mediated DNA base pair in tensegrity triangle

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	105.873, 105.873, 91.955
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.160 - 4.160
R-factor	0.2149
Rwork	0.212
R-free	0.24840
Structure solution method	SAD
RMSD bond length	0.017
RMSD bond angle	1.819
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	AutoSol
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.160	4.600
High resolution limit [Å]	4.160	4.160
Number of reflections	2035	192
<I/σ(I)>	11.4
Completeness [%]	86.8
Redundancy	9.9
CC(1/2)	0.999	0.190

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8.5	293	Tris, Magnesium sulfate, silver nitrate