7SLG

[T:Ag+:T--pH 11] Metal-mediated DNA base pair in tensegrity triangle

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	106.760, 106.760, 92.105
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.320 - 5.100
R-factor	0.1735
Rwork	0.172
R-free	0.20190
Structure solution method	SAD
RMSD bond length	0.013
RMSD bond angle	1.428
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	AutoSol
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall
Low resolution limit [Å]	65.250
High resolution limit [Å]	5.100
Number of reflections	1072
<I/σ(I)>	4.3
Completeness [%]	83.6
Redundancy	9.5
CC(1/2)	0.997

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	11	293	Tris, Magnesium sulfate, silver nitrate