7SLE
[T:Ag+:T--pH 10] Metal-mediated DNA base pair in tensegrity triangle
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-18 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | H 3 |
Unit cell lengths | 106.370, 106.370, 93.257 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.370 - 4.390 |
R-factor | 0.2183 |
Rwork | 0.217 |
R-free | 0.24120 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.034 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | AutoSol |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.370 | 4.880 |
High resolution limit [Å] | 4.390 | 4.390 |
Number of reflections | 1863 | 208 |
<I/σ(I)> | 13.6 | |
Completeness [%] | 74.8 | |
Redundancy | 10.6 | |
CC(1/2) | 1.000 | 0.405 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 10 | 293 | Tris, Magnesium sulfate, silver nitrate |